API 936 flashcards
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- Low-cement castable CaO range
- Low-cement castables contain 1.0 to 2.5 percent calcium oxide by weight, while ultra-low-cement castables contain 0.2 to 1.0 percent calcium oxide.
- Conventional castable CaO threshold
- Conventional castables contain more than 2.5 percent calcium oxide by weight, which lowers refractoriness and increases porosity compared with low-cement castables.
- No-cement castable definition
- No-cement castables contain less than 0.2 percent calcium oxide and rely on other bonding systems such as hydratable alumina or colloidal silica.
- Abrasion resistance in FCC
- Abrasion resistance of monolithic refractory increases with higher bulk density, lower apparent porosity, harder aggregate, and a stronger aggregate-matrix bond.
- Silica attack by vanadium
- Vanadium and sodium in FCC feed flux silica-containing refractories, so high-alumina or spinel refractories are selected for erosive and chemical service.
- Thermal conductivity versus density
- For dense monolithic refractories, thermal conductivity generally increases with bulk density and decreases with rising service temperature.
- Spinel refractory benefit
- Alumina-spinel castables resist thermal shock and slag attack because spinel has low thermal expansion and resists alkali and iron oxide penetration.
- Hexmesh anchor typical spacing
- Hexagonal mesh anchors are commonly on 2-inch centers, 3/4 to 1 inch deep, and 12 to 14 gauge stainless steel for dense monolithic linings.
- Anchor alloy temperature limit
- Type 304 stainless anchors suit oxidizing service to about 1500°F, type 310 to about 1900°F, and nickel alloys for higher or reducing service.
- Anchor hot-face clearance
- Anchor tips should terminate roughly 1/2 to 1 inch below the hot face so the refractory covers and protects the metal from overheating.
- Expansion joint purpose
- Expansion joints relieve thermal growth in castable linings; they are placed at regular intervals and at shell discontinuities to prevent random cracking.
- Lining thickness tolerance
- Installed monolithic lining thickness is typically checked against specification tolerance, commonly plus or minus 1/4 inch unless the project specifies tighter limits.
- Shell temperature design limit
- Refractory and insulation thickness are chosen to keep the steel shell below its design temperature, often about 500 to 650°F in FCC service.
- Mixing water temperature
- Clean mixing water should be about 50 to 80°F; hot water accelerates setting and cold water slows it, both altering working time and strength.
- Castable working time
- Working time is the period after mixing during which the castable can be placed and vibrated; it shortens as ambient and mix temperature rise.
- Vibration of castable
- Castable is consolidated with internal vibrators until air bubbles stop and the surface turns glossy; over-vibration causes segregation.
- Gunning rebound rule
- Rebound material that bounces off the target must never be reused or worked back into the lining because it lacks fines and bond.
- Curing low-cement castable
- Low-cement castables are typically moist-cured for about 24 hours at 65 to 85°F before dryout to allow hydraulic bond development.
- Test panel requirement
- Test panels are cast from the same mix and at the same time as field placement, then cured and dried with the lining for quality testing.
- Cold weather installation limit
- Refractory installation should not proceed when the shell or ambient temperature is below 50°F unless heating and enclosures maintain proper curing conditions.
- Cold crushing strength test
- Cold crushing strength is measured on cured and dried cube specimens, usually 2-inch cubes, per ASTM C133 to verify material strength.
- Bulk density acceptance
- Bulk density of field samples is commonly required to be within about 5 percent of the manufacturer's published value for the same product.
- Hammer tap inspection
- Hammer tapping detects voids, delamination, and unbonded refractory by a change from a sharp ring to a dull thud.
- Permanent linear change test
- Permanent linear change measures irreversible dimensional change after reheating a specimen to a specified temperature and cooling it.
- Abrasion resistance test
- Abrasion resistance is evaluated by ASTM C704, which blasts a specified abrasive at a refractory surface and measures volume loss.
- Anchor weld inspection sampling
- Anchor welds are inspected visually and by bend testing samples; failed welds require repair and re-inspection before lining placement.
- Moisture before dryout
- Residual moisture in a new lining should be checked and documented before dryout; excessive water can cause steam spalling during heat-up.
- Material storage requirement
- Cement-bonded castables are stored dry, off the ground, and within shelf life; bagged material that has caked or hardened is rejected.
- Dryout hold at 250°F
- A typical dryout holds at about 250 to 300°F to remove free water slowly before raising temperature further, preventing steam spalling.
- Dryout heating rate
- Dense castable linings are commonly heated at 25 to 50°F per hour during initial dryout, with slower rates for thick or low-permeability sections.
- Chemical water release
- Chemically bound water in cement-bonded refractories is driven off roughly between 500 and 900°F, requiring a controlled hold in that range.
- Repair area preparation
- Repairs require removal of all cracked, spalled, or unbonded material to sound refractory, with square edges and clean exposed anchors.
- Anchor replacement criterion
- Anchors that are severely oxidized, deformed, or have failed welds are replaced rather than embedded in new refractory.
- Crack repair threshold
- Cracks wider than about 1/8 inch or deep cracks that reach anchors are typically cut out and repaired during turnaround maintenance.
- Dryout vent purpose
- Vents or weep holes in a lining allow steam and water vapor to escape during dryout, reducing pressure buildup and spalling risk.